本书为双语版"国家级实验教学示范中心·中药学实验系列教材"之一。全书共分5章。第一章主要介绍分析化学实验基本要求，第二章主要介绍分析化学实验基本操作，第三章包括20个化学分析实验，第四章包括17个仪器分析实验，第五章包括2个设计性实验和1个综合性实验。本教材在编写过程中结合分析化学实验双语教学实践的经验，既满足学生个性发展需要，又注重培养学生分析问题、解决问题的能力。
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目录
- 目录
编写说明
第一章 分析化学实验基本要求 (1)
1.1 实验室安全常识 (1)
1.1.1 实验室安全规则 (1)
1.1.2 实验室安全标志 (2)
1.2 实验记录与实验报告 (2)
1.2.1 实验记录和实验报告注意事项 (2)
1.2.2 实验报告内容 (2)
1.3 化学试剂的一般知识 (3)
1.3.1 化学试剂的规格 (3)
1.3.2 分析用纯水 (3)
1.4 常用辞典、手册及网上信息查询简介 (4)
1.4.1 辞典、手册 (4)
1.4.2 网上信息查询 (4)
第二章 分析化学实验基本操 (5)
2.1 称量 (5)
2.1.1 分析天平 (5)
2.1.2 称量方法 (5)
2.2 玻璃仪器 (5)
2.2.1 放璃仪器的洗涤与干燥 (6)
2.2.2 玻璃仪器的使用 (7)
第三章 化学分析实验 (10)
实验3.1 氯化锁干燥失重的测定 (10)
实验3.2 生药灰分的测定 (11)
实验3.3 氢氧化锦标准溶液的配制和标定 (12)
实验3.4 食用醋分析 (14)
实验3.5 草酸含量测定 (15)
实验3.6 盐酸标准溶液的配制与标定 (17)
实验3.7 碳酸盐和碳酸氢盐的含量测定 (18)
实验3.8 混合碱的含量测定 (19)
实验3.9 高氯酸标准溶液的配制与标定 (21)
实验3.10 乳酸铺注射液中的乳酸铺含量测定 (22)
实验3.11 EDTA标准溶液的配制与标定（24）
实验3.12 水的硬度测定（25）
实验3.13 明矶中硫酸铝饵的含量测定 (27)
实验3.14 硫代硫酸铀标准溶液的配制与标定 (29)
实验3.15 腆标准榕液的配制与标定 (31)
实验3.16 腆量法测定维生素C的含量 (32)
实验3.17 高锺酸饵标准榕液的配制与标定 (34)
实验3.18 市售过氧化氢溶液的含量测定 (35)
实验3.19 硝酸银标准溶液和硫氨酸镀标准溶液的配制和标定 (37)
实验3.20 法杨斯法测定氯化物 (39)
第四章 仪器分析实验 (41)
实验4.1 阿司匹林片剂中乙酷水杨酸的含量测定 (41)
实验4.2 永停滴定法测定磺胶喃睫的含量 (43)
实验4.3 柱色谱法测定氧化铝活度 (44)
实验4.4 柱色谱法分离菠菜中的植物色素 (4的
实验4.5 黄连药材的薄层色谱鉴别 (48)
实验4.6 邻硝基苯胶和对硝基苯胶的薄层分离 (49)
实验4.7 氨基酸的纸包谱鉴别 (50)
实验4.8 气相色谱法测定町剂中乙醇的含量 (52)
实验4.9 高效液相色谱柱的性能考察及分离度测试 (53)
实验4.10 高效液相色谱法测定槐米中芦丁的含量 (55)
实验4.11 维生素B2注射液的定性鉴别及定量分析 (57)
实验4.12 荧光分光光度法测定维生素B2片中核黄素的含量 (58)
实验4.13 感冒冲剂中铜含量的测定 (60)
实验4.14 红外分光光度法测定苯甲酸和苯甲醇的结构 (61)
实验4.15 核磁共振波谱法测定水杨酸甲醋的结构 (63)
实验4.16 气相色谱质谱联用技术对混合物中甲苯、氯苯和澳苯定性分析 (65)
实验4.17 液相色谱质谱联用技术对中药黄苓中黄苓昔的定性和定量分析 (66)
第五章 设计性实验和综合性实验 (69)
实验5.1 胆矶中硫酸铜的含量测定(设计性实验) (69)
实验5.2 中药牲丹皮中丹皮酣的含量测定(设计性实验) (70)
实验5.3 大黄中蓝眼类化合物的柱色谱分离及组分的薄层鉴定(综合性实验) (70)
附录 (72)
附录一 相对原子质量表(1995年IUPAC) (72)
附录三 常用缓冲溶液 (73)
附录三 常用酸碱指示剂 (73)
附录四 常用酸碱的理度、含量和浓度 (74)
Table of Contents
Chapter 1 Laboratory General Knowledge (75)
1.1 Laboratory Safety (75)
1.1.1 Safety Rules (75)
1.1.2 Safety Signs (76)
1.2 The Laboratory Notebook (76)
1.2.1 Experiment Results Recording Policies (76)
1.2.2 Contents of a Laboratory Notebook (77)
1.3 Reagents (77)
1.3.1 Grades of Chemicals (77)
1.3.2 Grades of Purified Water (78)
1.4 Commonly Used DictionariestManuals and on-line Informations (78)
1.4.1 Dictionaries and Manuals (78)
1.4.2 On-line Informations (78)
Chapter 2 Experimental Techniques (79)
2.1 Weighing (79)
2.1.1 Analytical Balance (79)
2.1.2 Weighing Methods (79)
2.2 Glassware (80)
2.2.1 Cleaning and Drying Glassware (81)
2.2.2 Use of Volumetric Glassware (81)
Chapter 3 Chemical Analysis (86)
Experiment 3.1 Determination of Drying Loss in Barium Chloride (86)
Experiment 3.2 Determination of the Ash Content in the Crude Drug (87)
Experiment 3.3 Preparation and Standardization of Sodium Hydroxide Solution (88)
Experiment 3.4 Titration of a Commercial Vinegar Product (90)
Experiment 3.5 Analysis of the Oxalic Acid (91)
Experiment 3.6 Preparation and Standardization of Hydrochloride Acid Solution (93)
Experiment 3.7 Analysis of a Mixture of Carbonate and Bicarbonate (94)
Experiment 3.8 Titration of a Mixed &se (96)
Experiment 3.9 Preparation and Standardization of Perchloride Acid Solution (97)
Experiment 3.10 Determination of the Sodium Lactate in Sodium Lactate Injection (99)
Experiment 3.11 Preparation and Standardization of EDTA Solution (100)
Experiment 3.12 Determination of the Water Hardness (102)
Experiment 3.13 IRtermination of the Aluminum Potassium Su1fate in Alum (104)
Experiment 3.14 prepration and Standardization of Sodium Thiosulfate Solution (105)
Experiment 3.15 Preparation and Standardization of Iodine Solution (107)
Experiment 3.16 Iodimetric Titration of Vitamin C (109)
Experiment 3.17 Preparation and Standardization of Potassium Permanganate Solution (111)
Experiment 3.18 Determination of the Commercial Hydrogen Peroxide Solution (112)
Experiment 3.19 Preparation and Standardization of the Silver Nitrate Solution and Ammonium Thiocyanate solution (114)
Experiment 3.20 Fajans Determination of Chloride (116)
Chapter 4 Instrumental Analysis (118)
Experiment 4.1 IRtermination of the Acetylsalicylic Acid in Aspirin Tablet (118)
Experiment 4.2 Determination of Sulfadiazine with Dead-Stop Titration (120)
Experiment 4.3 Evaluation of the Activity Grade for A1uminum Oxide Powder by Column Chromatography (121)
Experiment 4.4 Separating Plant Pigments from Spinach Extract by Column Chromatography (123)
Experiment 4.5 The Identification of Rhizoma Coptidis by Thin Layer Chromatography (125)
Experiment 4.6 Separation of ortho-Nitroaniline and para-Nitroaniline by Thin Layer Chromatography (127)
Experiment 4.7 Identification of Amino acids by Paper Chromatography (128)
Experiment 4.8 Determination of Alcohol in Tincture by Gas Chromatography (130)
Experiment 4.9 Evaluation of the Performance of HPLC Column and IRtermination of Resol ution (132)
Experiment 4.10 Determination of Rutin in Flos Sophorae Immaturus by HPLC (134)
Experiment 4.11 Qualitative and Quantitative analysis of Vitamin~2 Injection (136)
Experiment 4.12 Analysis of Ribof1avin in a Vitamin Tablet by Fluorescence Spectrometry (137)
Experiment 4.13 The Assay of Cuprum in the Cold Medicine (139)
Experiment 4.14 Determination of Benzoic Acid and Benzoic Alcohol by IR Spectrophotometry (141)
Experiment 4.15 Determination of the Structure of Methyl Salicylate by NMR (142)
Experiment 4.16 Quantitative Analysis of Toluene Chlorobenzene and Bromobenzene in a Mixture with Gas Chromatography-Mass Spectrometry Hyphenated Technology (145)
Experiment 4.17 Qualitative and Quantitative Analysis of Baicalin in Radix Scutellariae with Liquid Chromatography-Mass Spectrometry Hyphenated Technology (146)
Chapter 5 Comprehensive and Designable Experiments (150)
Experiment 5.1 Determination of Copper Sulfate in Chalcanthite (Designable Experiment) (150)
Experiment 5.2 Determination of Paeonol in Cortex Moutan (Designable Experiment) (151)
Experiment 5.3 The Separation of Anthraquinone from Radix et Rhizome Rhei by Column Chromatography and the Identification of the Eluted Constituents by Thin Layer Chromatography (Comprehensive Experiment) (151)
Appendix (154)
Appendix 1 Table of Standard Atomic Weights(1995,IUPAC) (154)
Appendix 2 Commonly Used Buffer Solution (155)
Appendix 3 Commonly Used Acid-&se Indicator (155)
Appendix 4 Commonly Used Acid-Base Density，Content and Concentration (156)
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