编写说明 第一章 分析化学实验基本要求 1.1 实验室安全常识 1.1.1 实验室安全规则 1.1.2 实验室安全标志 1.2 实验记录与实验报告 1.2.1 实验记录和实验报告注意事项 1.2.2 实验报告内容 1.3 化学试剂的一般知识 1.3.1 化学试剂的规格 1.3.2 分析用纯水 1.4 常用辞典、手册及网上信息查询简介 1.4.1 辞典、手册 1.4.2 网上信息查询 第二章 分析化学实验基本操作 2.1 称量 2.1.1 分析天平 2.1.2 称量方法 2.2 玻璃仪器 2.2.1 玻璃仪器的洗涤与干燥 2.2.2 玻璃仪器的使用 第三章 化学分析实验 实验3.1 氯化钡干燥失重的测定 实验3.2 生药灰分的测定 实验3.3 氢氧化钠标准溶液的配制和标定 实验3.4 食用醋分析 实验3.5 草酸含量测定 实验3.6 盐酸标准溶液的配制与标定 实验3.7 碳酸盐和碳酸氢盐的含量测定 实验3.8 混合碱的含量测定 实验3.9 高氯酸标准溶液的配制与标定 实验3.10 乳酸钠注射液中的乳酸钠含量测定 实验3.11 EDTA标准溶液的配制与标定 实验3.12 水的硬度测定 实验3.13 明矾中硫酸铝钾的含量测定 实验3.14 硫代硫酸钠标准溶液的配制与标定 实验3.15 碘标准溶液的配制与标定 实验3.16 碘量法测定维生素C的含量 实验3.17 高锰酸钾标准溶液的配制与标定 实验3.18 市售过氧化氢溶液的含量测定 实验3.19 硝酸银标准溶液和硫氰酸铵标准溶液的配制和标定 实验3.20 法杨斯法测定氯化物 第四章 仪器分析实验 实验4.1 阿司匹林片剂中乙酰水杨酸的含量测定 实验4.2 永停滴定法测定磺胺嘧啶的含量 实验4.3 柱色谱法测定氧化铝活度 实验4.4 柱色谱法分离菠菜中的植物色素 实验4.5 黄连药材的薄层色谱鉴别 实验4.6 邻硝基苯胺和对硝基苯胺的薄层分离 实验4.7 氨基酸的纸色谱鉴别 实验4.8 气相色谱法测定酊剂中乙醇的含量 实验4.9 高效液相色谱柱的性能考察及分离度测试 实验4.10 高效液相色谱法测定槐米中芦丁的含量 实验4.11 维生素B12注射液的定性鉴别及定量分析 实验4.12 荧光分光光度法测定维生素B2片中核黄素的含量 实验4.13 感冒冲剂中铜含量的测定 实验4.14 红外分光光度法测定苯甲酸和苯甲醇的结构 实验4.15 核磁共振波谱法测定水杨酸甲酯的结构 实验4.16 气相色谱-质谱联用技术对混合物中甲苯、氯苯和溴苯定性分析 实验4.17 液相色谱-质谱联用技术对中药黄芩中黄芩苷的定性和定量分析 第五章 设计性实验和综合性实验 实验5.1 胆矾中硫酸铜的含量测定（设计性实验） 实验5.2 中药牡丹皮中丹皮酚的含量测定（设计性实验） 实验5.3 大黄中蒽醌类化合物的柱色谱分离及组分的薄层鉴定（综合性实验） 附录 附录一 相对原子质量表（1995年，IUPAC） 附录二 常用缓冲溶液 附录三 常用酸碱指示剂 附录四 常用酸碱的密度、含量和浓度 Chapter 1 Laboratory General Knowledge 1.1 Laboratory Safety 1.1.1 Safety Rules 1.1.2 Safety Signs 1.2 The Laboratory Notebook 1.2.1 Experiment Results Recording Policies 1.2.2 Contents of a Laboratory Notebook 1.3 Reagents 1.3.1 Grades of Chemicals 1.3.2 Grades of Purified Water 1.4 Commonly Used Dictionaries，Manuals and on-line Informations 1.4.1 Dictionaries and Manuals 1.4.2 On-line Informations Chapter 2 Experimental Techniques 2.1 Weighing 2.1.1 Analytical Balance 2.1.2 Weighing Methods 2.2 Glassware 2.2.1 Cleaning and Drying Glassware 2.2.2 Use of Volumetric Glassware Chapter 3 Chemical Analysis Experiment 3.1 Determination of Drying Loss in Barium Chloride Experiment 3.2 Determination of the Ash Content in the Crude Drug Experiment 3.3 Preparation and Standardization of Sodium Hydroxide Solution Experiment 3.4 Titration of a Commercial Vinegar Product Experiment 3.5 Analysis of the Oxalic Acid Experiment 3.6 Preparation and Standardization of Hydrochloride Acid Solution Experiment 3.7 Analysis of a Mixture of Carbonate and Bicarbonate Experiment 3.8 Titration of a Mixed Base Experiment 3.9 Preparation and Standardization of Perchloride Acid Solution Experiment 3.10 Determination of the Sodium Lactate in Sodium Lactate Injection Experiment 3.11 Preparation and Standardization of EDTA Solution Experiment 3.12 Determination of the Water Hardness Experiment 3.13 Determination of the Aluminum Potassium Sulfate in Alum Experiment 3.14 Preparation and Standardization of Sodium Thiosulfate Solution Experiment 3.15 Preparation and Standardization of Iodine Solution Experiment 3.16 Iodimetric Titration of Vitamin C Experiment 3.17 Preparation and Standardization of Potassium Permanganate Solution Experiment 3.18 Determination of the Commercial Hydrogen Peroxide Solution Experiment 3.19 Preparation and Standardization of the Silver Nitrate Solution and Ammonium Thiocyanate solution Experiment 3.20 Fajans Determination of Chloride Chapter 4 Instrumental Analysis Experiment 4.1 Determination of the Acetylsalicylic Acid in Aspirin Tablet Experiment 4.2 Determination of Sulfadiazine with Dead-Stop Titration Experiment 4.3 Evaluation of the Activity Grade for Aluminum Oxide Powder by Column Chromatography Experiment 4.4 Separating Plant Pigments from Spinach Extract by Column Chromatography Experiment 4.5 The Identification of Rhizoma Coptidis by Thin Layer Chromatography Experiment 4.6 Separation of ortho-Nitroaniline and para-Nitroaniline by Thin Layer Chromatography Experiment 4.7 Identification of Amino acids by Paper Chromatography Experiment 4.8 Determination of Alcohol in Tincture by Gas Chromatography Experiment 4.9 Evaluation of the Performance of HPLC Column and Determination of Resolution Experiment 4.10 Determination of Rutin in Flos Sophorae Immaturus by HPLC Experiment 4.11 Qualitative and Quantitative analysis of Vitamin B12 Injection Experiment 4.12 Analysis of Riboflavin in a Vitamin B2 Tablet by Fluorescence Spectrometry Experiment 4.13 The Assay of Cuprum in the Cold Medicine Experiment 4.14 Determination of Benzoic Acid and Benzoic Alcohol by IR Spectrophotometry Experiment 4.15 Determination of the Structure of Methyl Salicylate by NMR Experiment 4.16 Quantitative Analysis of Toluene，Chlorobenzene and Bromobenzene in a Mixture with Gas Chromatography-Mass Spectrometry Hyphenated Technology Experiment 4.17 Qualitative and Quantitative Analysis of Baicalin in Radix Scutellariae with Liquid Chromatography-Mass Spectrometry Hyphenated Technology Chapter 5 Comprehensive and Designable Experiments Experiment 5.1 Determination of Copper Sulfate in Chalcanthite （Designable Experiment） Experiment 5.2 Determination of Paeonol in Cortex Moutan （Designable Experiment） Experiment 5.3 The Separation of Anthraquinone from Radix et Rhizome Rhei by Column Chromatography and the Identification of the Eluted Constituents by Thin Layer Chromatography （Comprehensive Experiment） Appendix Appendix 1 Table of Standard Atomic Weights（1995，IUPAC） Appendix 2 Commonly Used Buffer Solution Appendix 3 Commonly Used Acid-Base Indicator Appendix 4 Commonly Used Acid-Base Density，Content and Concentration
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